Microwave plasma sintering of porous nanosized CHA/β-TCP biphasic bioceramics

Ran Xu

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Microwave plasma sintering of porous nanosized CHA/β-TCP biphasic bioceramics

更新时间：2023-11-28

- Microwave plasma sintering of porous nanosized CHA/β-TCP biphasic bioceramics
- Advanced Engineering Sciences Vol. 40, Issue 4, Pages: 100-104(2008)
- 作者机构：
  
  四川大学轻纺与食品学院
- 作者简介：
- 基金信息：
- DOI：
  CLC：
- Published：2008，
  
  Published Online：28 May 2008，
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冉旭.微波等离子体烧结制备多孔纳米CHA/β-TCP双相生物陶瓷[J].工程科学与技术,2008,40(4):100-104.

Ran Xu. Microwave plasma sintering of porous nanosized CHA/β-TCP biphasic bioceramics. [J]. Advanced Engineering Sciences 40(4):100-104(2008)
冉旭.微波等离子体烧结制备多孔纳米CHA/β-TCP双相生物陶瓷[J].工程科学与技术,2008,40(4):100-104. DOI：

Ran Xu. Microwave plasma sintering of porous nanosized CHA/β-TCP biphasic bioceramics. [J]. Advanced Engineering Sciences 40(4):100-104(2008) DOI：

摘要

中文摘要: 为了提高钙磷陶瓷材料性能，以含碳酸化羟基磷灰石纳米粉体（CHA）为原料，采用含水蒸汽CO2微波等离子体快速烧结新技术阻止CHA分解和实现多孔CHA /β-TCP双相生物陶瓷的纳米化。在优化工艺条件下，制得了平均晶粒尺寸为92nm，气孔率为55.9％，CO2含量为4％左右，压缩强度为13.7 MPa的多孔纳米TCP/CHA双相生物陶瓷。与常规马弗炉烧结相比，微波等离子体烧结时间缩短，烧结温度降低，能有效阻止CHA分解，提高了烧结效率。微波等离子体烧结是一种快速制备纳米生物陶瓷的有效方法。

Abstract

Abstract:Porous nanosized CHA/β-TCP biphasic bioceramics were prepared by microwave plasma sintering in a wet carbon dioxide atmosphere to improve its biological and mechanical performance. Through the optimization of sintering parameters including the sintering temperature and the holding time

porous bioceramics with average crystal size of 92nm

porosity of 55.9%

CO32- content of 4wt% and compressive strength of 13.7MPa were obtained. The comparison between conventional sintered specimens and microwave plasma sintered specimens showed that the latter exhibit smaller crystal size and higher carbonate content and compressive strength. Microwave plasma sintering is a promising method of preparing nanosized bioceramics.

关键词

碳酸化羟基磷灰石磷酸三钙双相钙磷生物陶瓷微波等离子烧结

Keywords

carbonated hydroxyapatiteβ-TCPbioceramicsmicrowave plasma sintering

references

Grimm B,Miles A W,Turner I G,Optimizing a hydroxyapatite/tricalcium-phosphate ceramic as a bone graft extender for impaction grafting,Journal of Materials Science:Materials in Medicine,2001(10-12).

LeGeros R Z,Lin S,Rohanizadeh R,Biphasic calcium phosphate bioceramics:preparation,properties and applications,Journal of Materials Science:Materials in Medicine,2003(3).

Daculsi G,Laboux O,Malard O,Current state of the art of biphasic calcium phosphate bioceramics,Journal of Materials Science:Materials in Medicine,2003(3).

Landi E,Tampieri A,Celotti G,Nucleation of biomimetic apatite in synthetic body fluids:dense and porous scaffold development,Biomaterials,2005(16).

Doi Y,Shibutani T,Moriwaki Y,Sintered carbonate apatites as bioresorbable bone substitute,Journal of Biomedical Materials Research,1998(4).

Barralet J,Akao M,Aoki H,Dissolution of dense carbonate apatite subcutaneously implanted in wistar rats,Journal of Biomedical Materials Research,2000(2).

Hazegawa M,Doi Y,Uchida A,Cell-mediated bioresorption of sintered carbonate apatite in rabbits,Journal of Bone and Joint Surgery-British Volume,2003(B).

Barralet J E,Aldred S,Wright A J,In vitro behavior of albumin-loaded carbonate hydroxyapatite gel,Journal of Biomedical Materials Research,2002(3).

Barralet J E,Best S M,Bonfield W,Effect of sintering parameters on the density and microstructure of carbonate hydroxyapatite,Journal of Materials Science:Materials in Medicine,2000(11).

Peng J H,Hong PJ,Dai SS,Microwave plasma sintering of nanocrystalline alumina,Journal of Materials Science and Technology,1998(2).

Bengisu M,Inal O T,Sintering of MgO and MgO-TiC ceramics by plasma,microwave and conventional heating,Journal of Materials Science,1994(20).

蔡杰,李包顺,庄汉锐,微波等离子体技术在高技术新材料领域的应用,材料导报,1995(2).

季金苟.冉均国.苟立.王方瑚.孙璐薇微波等离子体烧结多孔HA/β-TCP双相生物陶瓷的研究 [J].

Oh S T,Tajima K I,Ando M,Fabrication of porous Al2O3 by microwave sintering and its properties,Materials Letters,2001(3-4).

Murugan R,Ramakrishna S,Production of ultra-fine bioresorbable carbonated hydroxyapatite,Acta Biomaterialia,2006(2).

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